A NEW TRICYCLIC SULFUR-RICH PHOSPHANE
| Autor(en): | BLACHNIK, R LONNECKE, P |
Stichwörter: | (T-BU(S)P)2P4S3; (T-BUP)(T-BU(S)P)P4S3; (T-BUP)2P4S3; Chemistry; Chemistry, Inorganic & Nuclear; P-31 NMR DATA; PHOSPHORUS; PREPARATION | Erscheinungsdatum: | 1994 | Herausgeber: | JOHANN AMBROSIUS BARTH VERLAG | Journal: | ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | Volumen: | 620 | Ausgabe: | 1 | Startseite: | 167 | Seitenende: | 172 | Zusammenfassung: | From the products of the reaction of P4S3 with tert-Butyliodide the compound (t-Bu(S)P)2P4S3 was isolated in low yield. The compound is stable and has a structure related to the hydrocarbon brexane. By reaction with triphenylphosphin the compounds (t-BuP)(t-Bu(S)P)P4S, and (t-BUP)2P4S3 were obtained. The P-31-nmr spectra of all compounds were solved and used to determine the structure of the molecules. A complete set of P-31-nmr data is given. |
ISSN: | 00442313 | DOI: | 10.1002/zaac.19946200127 |
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