A NEW TRICYCLIC SULFUR-RICH PHOSPHANE

Autor(en): BLACHNIK, R
LONNECKE, P
Stichwörter: (T-BU(S)P)2P4S3; (T-BUP)(T-BU(S)P)P4S3; (T-BUP)2P4S3; Chemistry; Chemistry, Inorganic & Nuclear; P-31 NMR DATA; PHOSPHORUS; PREPARATION
Erscheinungsdatum: 1994
Herausgeber: JOHANN AMBROSIUS BARTH VERLAG
Journal: ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
Volumen: 620
Ausgabe: 1
Startseite: 167
Seitenende: 172
Zusammenfassung: 
From the products of the reaction of P4S3 with tert-Butyliodide the compound (t-Bu(S)P)2P4S3 was isolated in low yield. The compound is stable and has a structure related to the hydrocarbon brexane. By reaction with triphenylphosphin the compounds (t-BuP)(t-Bu(S)P)P4S, and (t-BUP)2P4S3 were obtained. The P-31-nmr spectra of all compounds were solved and used to determine the structure of the molecules. A complete set of P-31-nmr data is given.
ISSN: 00442313
DOI: 10.1002/zaac.19946200127

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