Crystal structure of pentachloro(3,3 `-thiodipropionitrile)tantalum(V), TaCl5[NC(CH2)(2)S(CH2)(2)CN] and of pentachloro(3,3 `-thiodipropionitrile)niobium(V), NbCl5[NC(CH2)(2)S(CH2)(2)CN]
| Autor(en): | Ibrahim-Abdelhalim-Ahmed Blachnik, R Reuter, H Stumpf, K |
Stichwörter: | Crystallography | Erscheinungsdatum: | 1999 | Herausgeber: | WALTER DE GRUYTER GMBH | Journal: | ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | Volumen: | 214 | Ausgabe: | 1 | Startseite: | 117 | Seitenende: | 118 | Zusammenfassung: | C6H8Cl5N2STa, monoclinic, P12(1)/n1 (No. 14), a = 8.051(3) Angstrom, b = 9.430(2) Angstrom, c = 18.293(5) Angstrom, beta = 100.32(3)degrees, V = 1366.4 Angstrom(3) Z = 4, R-gt(F) = 0.031, R-w(F-2) = 0.073, T = 223 K. C6H8Cl5N2NbS, monoclinic, P12(1)/n1 (No. 14), a = 8.069(1) Angstrom, b = 9.4689(9) Angstrom, c = 18.440(2) Angstrom, beta = 100.19(1)degrees, V = 1386.7 Angstrom(3), Z = 4, R-gt(F) = 0.020, R-w(F-2) = 0.057, T = 293 K. |
ISSN: | 14337266 |
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