Crystal structure of pentachloro(3,3′-thiodipropionitrile)tantalum(V), TaCl5[NC(CH2)2S(CH2)2 CN] and of pentachloro(3,3′-thiodipropionitrile)niobium(V), NbCl5[NC(CH2)2S(CH2)2 CN]

Crystal structure of pentachloro(3,3′-thiodipropionitrile)tantalum(V), TaCl₅[NC(CH₂)₂S(CH₂)₂CN] and of pentachloro(3,3′-thiodipropionitrile)niobium(V), NbCl₅[NC(CH₂)₂S(CH₂)₂CN]

Autor(en):	Ibrahim-Abdelhalim-Ahmed Blachnik, R Reuter, H Stumpf, K
Stichwörter:	Crystallography
Erscheinungsdatum:	1999
Herausgeber:	WALTER DE GRUYTER GMBH
Journal:	ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
Volumen:	214
Ausgabe:	1
Startseite:	117
Seitenende:	118
Zusammenfassung:	C6H8Cl5N2STa, monoclinic, P12(1)/n1 (No. 14), a = 8.051(3) Angstrom, b = 9.430(2) Angstrom, c = 18.293(5) Angstrom, beta = 100.32(3)degrees, V = 1366.4 Angstrom(3) Z = 4, R-gt(F) = 0.031, R-w(F-2) = 0.073, T = 223 K. C6H8Cl5N2NbS, monoclinic, P12(1)/n1 (No. 14), a = 8.069(1) Angstrom, b = 9.4689(9) Angstrom, c = 18.440(2) Angstrom, beta = 100.19(1)degrees, V = 1386.7 Angstrom(3), Z = 4, R-gt(F) = 0.020, R-w(F-2) = 0.057, T = 293 K.
ISSN:	1433-7266

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